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Poster
Selective Silylation of ß-Cyclodextrin
University of West Florida Libraries
Summer Undergraduate Research Program (University of West Florida, Pensacola, Florida, 2021)
2021
Abstract
Sonication was used to silylate the seven primary alcohols of ß-cyclodextrin. The sonication reaction produced yields comparable to published procedures and reduced the time of silylation by 75% (1).
The reaction of ß-cyclodextrin and tert-Butyldimethylsilyl chloride in dry pyridine resulted in a 71% yield of Heptakis(6-O-tert-Butyldimethylsilyl)- ß-cyclodextrin.¹ H NMR and ¹³C NMR were used to characterize the product.
Details
- Title
- Selective Silylation of ß-Cyclodextrin
- Resource Type
- Poster
- Event
- Summer Undergraduate Research Program (University of West Florida, Pensacola, Florida, 2021)
- Contributors
- Dr. Ajay R. Lajmi (Faculty Mentor)
- Publisher
- University of West Florida Libraries; Argo Scholar Commons
- Format
- pdf
- Copyright
- Permission granted to the University of West Florida Libraries to digitize and/or display this item for non-profit research and educational purposes. Any reuse of this item in excess of fair use or other copyright exemptions requires the permission of the copyright holder.
- Identifiers
- 99380090299006600
- Academic Unit
- Summer Undergraduate Research Program 2021
- Language
- English